ASTM D5830-22

Standard Test Method for Solvents Analysis in Hazardous Waste Using Gas Chromatography

ACTIVE

About this standard

Languages
English
Type
ASTM
Status
ACTIVE
Publication date
01 March 2022
Withdrawn Date

About this training

Summary

< div class=" SectionLevel2" > < p class=" subsec1 cdone2" > < span class=" Head3 cdone" > 1.1< / span>  This test method is used to determine qualitatively and quantitatively the presence of the following compounds in waste samples using gas chromatography. This test method is intended for use as a screening method with a typical reporting level of 0.1 %.

< div class=" ParaCenter" > < table style=" border-collapse: collapse border-top-style:none border-bottom-style:none " class=" datatable gridtype" width=" 400px" > < col align=" left" width=" 200px" > < / col> < col align=" center" width=" 200px" > < / col> < tbody class=" cdone" > < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Dichodifluoromethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Tetrahydrofuran

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Trichlorofluoromethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Acetone

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_standard" > 1,1,2-Trichloro-1,2,2-
 trifluoroethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_standard" > Methyl Ethyl Ketone
MIBK

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Methanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Cyclohexanone

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethyl Acetate

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Isopropanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Propyl Acetate

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > < span class=" overriddenformat" style=" font-style:italic font-weight:normal " > n< / span> -Propanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Butyl Acetate

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Isobutanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Benzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > < span class=" overriddenformat" style=" font-style:italic font-weight:normal " > n< / span> -Butanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Toluene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > < span class=" overriddenformat" style=" font-style:italic font-weight:normal " > tert< / span> -Butanol

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethylbenzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Methylene Chloride

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Xylenes

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Chloroform

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Styrene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Carbon Tetrachloride

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Chlorobenzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,1-Dichloroethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Dichlorobenzenes

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,2-Dichloroethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Nitrobenzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,2-Dichloropropane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Fluorobenzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,1-Dichloroethylene

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > < span class=" overriddenformat" style=" font-style:italic font-weight:normal " > n< / span> -Propyl Benzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,2-Dichloroethene

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Isopropyl Benzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,1,1-Trichloroethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Isobutyl Benzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Tetrachloroethylene

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > < span class=" overriddenformat" style=" font-style:italic font-weight:normal " > n< / span> -Butyl Benzene

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Trichloroethylene

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 2-Ethoxyethanol

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Tetrachloroethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 2-Butoxyethanol

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Cyclopentane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 2-Ethoxyethanol Acetate

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Pentane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 2-Methoxyethanol

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Hexane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Bromoform

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Heptane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Carbitol

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Cyclohexane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethyl Ether

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > < span class=" overriddenformat" style=" font-style:italic font-weight:normal " > Iso< / span> octane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > 1,4-Dioxane

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Nitropropane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Diacetone Alcohol

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethanolamine

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Acetonitrile

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Nitromethane

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Pyridine

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethylene Chloride

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Toluidine

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Benzyl Chloride

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Ethylene Glycol

< / td> < / tr> < tr> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" >  

< / td> < td style=" vertical-align:top " > < p style=" text-align:left" class=" tablecell_indented" > Propylene Glycol

< / td> < / tr> < / tbody> < / table> < / div> < div class=" SectionLevel3" > < p class=" subsec2 cdone2" > < span class=" Head4 cdone" > 1.1.1< / span>  This compound list is a compilation of hazardous solvents and other constituents that are commonly seen in hazardous waste samples.

< / div> < / div> < div class=" SectionLevel2" > < p class=" subsec1 cdone2" > < span class=" Head3 cdone" > 1.2< / span>  The scope of this test method may be expanded to include other volatile and semivolatile organic constituents such as but not limited to those described below, provided the intended use data quality objectives including sampling, recovery, and analytic data quality are demonstrated as satisfied by the user.

< div class=" SectionLevel3" > < p class=" subsec2 cdone2" > < span class=" Head4 cdone" > 1.2.1< / span>  Hydrocarbon mixtures such as kerosene and mineral spirits.

< / div> < div class=" SectionLevel3" > < p class=" subsec2 cdone2" > < span class=" Head4 cdone" > 1.2.2< / span>  High-boiling organics, defined here as compounds which boil above < span style=" font-style:italic font-weight:normal " class=" overriddenformat" > n< / span> -Hexadecane.

< / div> < div class=" SectionLevel3" > < p class=" subsec2 cdone2" > < span class=" Head4 cdone" > 1.2.3< / span>  Other organics that the analyst is able to identify, either through retention time data or gas chromatography/ mass spectrometric (GC/ MS) analysis.

< / div> < / div> < div class=" SectionLevel2" > < p class=" caveat cdone2" > < span class=" Head3 cdone" > 1.3< / span>  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

< / div> < div class=" SectionLevel2" > < p class=" WTOcaveat cdone2" > < span class=" Head3 cdone" > 1.4< / span>  This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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